A synergetic effect of sonication with yolk-shell nanocatalyst for green synthesis of spirooxindoles
نویسندگان
چکیده
A synergetic effect of ultrasonic irradiation and yolk–shell nanocatalyst was examined for the synthesis spirooxindoles from isatin, malononitrile cyclohexanone. It found this contributory can be accelerated desired reaction toward obtaining highly pure products in excellent yields short times. The contains melamine anchored onto magnetic Fe3O4 nanoparticles were applied as active base catalyst sonication spirooxindole compounds. This has core very with great area surface shell. novel prepared through simple method characterized by using FT-IR spectrum, X-ray diffraction (XRD), scanning electron microscopy (SEM), thermo gravimetric analysis (TGA), Brunauer–Emmett–Teller (BET) vibrating sample magnetometer (VSM). used different derivatives under irradiation.
منابع مشابه
Nano-peanut shell-OSO3H: Green and natural-based renewable nanocatalyst for one-pot synthesis of dihydropyrano[3,2-b]chromenedione derivatives
Nano-peanut shell‑OSO3H nanoparticles were simply prepared and characterized by the scanning electron microscopy (SEM), transmission electron microscope (TEM), fourier transform infrared (FT-IR), energy dispersive X-ray spectroscopy (EDX), and thermal analysis techniques (TGA/DTG). The catalytic activity of nano-peanut shell‑OSO3H was studied in the synthesis of biological...
متن کاملassessment of the effect of honey as a topical therapy for intra oral wound healing in rat.
چکیده ندارد.
15 صفحه اولNanocrystalline MgAl2O4 as a Heterogeneous Nanocatalyst for the Synthesis of 2-Ketomethylquinolines Using Green Design Methodology
In this investigation, a facile and green sonochemical route has been developed for the synthesis of 2-Ketomethylquinolines by using 2-methylquinolines and several acyl chlorides in the presence of nanocrystalline MgAl2O4 as an efficient heterogeneous catalyst. The combination of nanocatalyst and ultrasonic process afforded corresponding ketomethyl quinolines in shorter re...
متن کاملH6P2W18O62: A Green and Reusable Catalyst for the One-pot Three-Component Synthesis of Spirooxindoles in Water
Wells–Dawson tungsten heteropolyacid (H6P2W18O62) has been applied as an effective heterogeneous catalyst for one-pot synthesis of spiro[4H-pyran-3,3’-oxindoles] via reaction of various isatins, malonitrile and 1,3-dicarbonyl compound in water. The corresponding products were obtained in high yields. The catalysts were easily recycled and reused without loss of their catalytic activity.
متن کاملsingle-step synthesis of multi-component spirobarbiturates using ionic liquids and synthesis of substituted pyridine filled with catalysts supported on solid substrate
in this thesis, a better reaction conditions for the synthesis of spirobarbiturates catalyzed by task-specific ionic liquid (2-hydroxy-n-(2-hydroxyethyl)-n,n-dimethylethanaminium formate), calcium hypochlorite ca(ocl)2 or n-bromosuccinimide (nbs) in the presence of water at room temperature by ultrasonic technique is provided. the design and synthesis of spirocycles is a challenging task becaus...
15 صفحه اولذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: Green Chemistry Letters and Reviews
سال: 2021
ISSN: ['1751-7192', '1751-8253']
DOI: https://doi.org/10.1080/17518253.2021.1921284